Spark plasma sintering of hydrothermally synthesized bismuth ferrite

Effect of High-Energy Ball Milling on the Magnetic Properties of NiZn Ferrite Ceramics Synthesized by Spark Plasma Sintering

High-density fine-grained Ni0.5Zn0.5Fe2O4 ferrite ceramics were synthesized by spark plasma sintering (SPS) in conjunction with high energy ball milling. The precursor powders were milled for 20 h, 40 h, and 60 h, respectively, and the milled powders were all sintered for 5 min at 900 ̊C. All the samples exhibit a single spinel phase. With increasing of the ball milling time, the relative densit...

New Mechanism for Ferroelectricity in the Perovskite Ca2-xMnxTi2O6 Synthesized by Spark Plasma Sintering.

Perovskite oxides hosting ferroelectricity are particularly important materials for modern technologies. The ferroelectric transition in the well-known oxides BaTiO3 and PbTiO3 is realized by softening of a vibration mode in the cubic perovskite structure. For most perovskite oxides, octahedral-site tilting systems are developed to accommodate the bonding mismatch due to a geometric tolerance f...

Spark Plasma Sintering of Negative Temperature Coefficient Thermistor Ceramics

Application of Spark Plasma Sintering for Manufacturing of Thermoelectric Materials

V-VI thermoelectric compounds like Bi2Te3-based alloys are well known for room temperature applications like Peltier coolers or thermogenerators. Their anisotropic physical properties and mechanical weakness are a problem for the manufacturing. To overcome the mechanical problem Spark Plasma Sintering (SPS) was used. 2 inch Wafers of polycrystalline bismuth telluride based n-type and p-type the...

Spark plasma sintering of ductile ceramic particles: study of LiF

Densification of cuboidal micrometer-sized lithium fluoride particles as ductile ceramic by spark plasma sintering (SPS) was investigated. Specimens were fabricated at different pressures and temperature conditions, ranging from 2 to 100 MPa at 500 C and from 200 to 700 C under 100 MPa of applied pressure, respectively. Dense specimens of 99 % relative density were fabricated by heating to 500 ...